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Orgo Esterification discussion

Submitted by bthoole on Wed, 11/14/2018 - 18:03

After the solution was refluxed to worked up to remove the water, the final product was analyzed using infrared spectroscopy. The spectroscopy analysis provided peaks that correspond to that of an ester, which is what was expected and can confirm the esterification process in the synthesis of 1-propyl propionate. The IR spectrum showed a peak just to the right of 3000 cm-1 at 2972.43 cm-1. This peak corresponds to the alkyl carbon-hydrogen bond in the ester. The stretch that starts at peak 1740.83 cm-1 is a measurement of the double bond between carbon and oxygen. These are the results that would be seen in a sample of pure ester, but the IR spectrum also gives peak values above 3000 cm-1, which suggests impurities containing a hydroxyl oxygen and hydrogen bond. The peak is highest at 3453.69 cm-1. This impurity could be a result of left-over water or a result of alcohol contamination from the 1-propanol.

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